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Johannsen, M. ; Schulze, U. ; Sahre, K. ; Komber, H. ; Voit, B.
Synthesis of allyl-terminated polar macromonomers by metallocene-catalyzed polymerizations of 10-undecene-1-ol

Poly(10-undecene-1-ol) macromonomers were synthesized by metallocene-catalyzed polymerization using vinyl chloride as a chain transfer agent. Using this technique, predominantly allyl terminated polymers could be obtained, which was verified by NMR spectroscopy and matrix-assisted laser desorption ionization time-of-flight mass spectrometry (MALDI-TOF-MS). By means of the mass spectra, a detailed interpretation of the nature of the head and end groups of these polymers was possible.

Source
ACS Macro Letters / American Chemical Society 1

Pages
352-355

DOI
http://dx.doi.org/10.1021/mz200185b

Published
January 2012
 
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